WKT-A9 Exquisite Karl Fischer Micro Moisture Analyzer with Card Furnace

NegotiableUpdate on 04/19

Model

Nature of the Manufacturer: Producers

Product Category

Place of Origin

Online Consult

Overview

The "Exquisite" Karl Fischer Micro Moisture Analyzer WKT-A9 uses the principle of Karl Fischer Coulombic Method (coulometric method) to quickly determine trace moisture in samples. The moisture content can be measured as low as 0.001ppm, and can determine the trace amounts of solids, liquids, and powders within 1 minute

Product Details

Product Details

product overview

Weike MeituoThe WKT-A9 "Exquisite" Karl Fischer Micro Moisture Analyzer utilizes the principle of Karl Fischer Coulombic Method (coulometric method) to quickly determine trace moisture in samples. The moisture content can be measured as low as 0.001ppm, and the micro moisture content of solids, liquids, and powders can be determined within 1 minute. The instrument has a built-in printing function and can store 500 sets of data, which can be queried and printed in real time! Innovative reminders and built-in electronic manuals make instrument operation no longer complicated. WKT-A9 complies with multiple national and international moisture measurement standards, with eight moisture calculation formulas and six measurement methods that can meet the needs of moisture measurement in various industries. It is widely used in industries such as chemical, petroleum, pharmaceutical, power, food, scientific research, and testing.

product operation

Operation steps:

Reagent debugging steps:

First, assemble the card type moisture analyzer and connect it to the power supply. Turn on the power switch

1. Add Karl Fischer titration reagent to the middle of the electrolytic cell scale line

2. Use a 100 microliter sampler to slowly inject distilled water or purified water

Wait for the color of the reagent to gradually fade

3. The color of the reagent has become lighter, and the instrument is displaying. Please wait for the instrument to stabilize before stopping the water injection

4. The instrument automatically electrolyzes the just added water, and after the electrolysis is completed, the instrument will indicate that the balance can be tested

Sample determination steps:

1. After sampling with an injector, place it on an analytical balance and weigh it. Click to remove the skin

2. After clicking on start measurement, inject the sample into the electrolytic cell bottle

3. Take out the sampler and place it on the analytical balance for weighing. The weight displayed on the balance at this time is the weight of the sample

4. Input the sample weight into the instrument and wait for measurement

5. The measurement is completed, and the instrument displays the measurement results and automatically stores them

The above measurement steps are only applicable to liquids and soluble solids, gases, insoluble solids, side reaction samples, and strong acid and alkali samples. Please feel free to contact us for solutions!

Product Features

Vicometo brandThe WKT-A9 "Exquisite" Karl Fischer Micro Moisture Analyzer has the following characteristics:
1. Automatic control of background current and current current, automatically deducting the influence of air or carrier gas moisture
2. The adjustable settings of electrolysis current and electrolysis endpoint can adapt to the sensitivity requirements of different samples for electrolysis
3. Gather eight moisture concentration display methods and six moisture measurement methods to meet your measurement needs for any sample
4. Multiple data display methods: sample weight, moisture content (μ g), measurement time ppm、%、 Sample number, electrolysis current, background current (caused by environmental or carrier gas interference) potential, measurement time, system time, operator number, in compliance with GLP experimental record standards
5. Can store 500 sets of data, automatically print after measurement, and track historical data for reference
6. Imported materials and components, instruments are stable, accurate, and durable
7. The data processing CPU uses imported chips from the United States to ensure stable and accurate instrument calculations
8. The color touch screen operating system is like a mobile app that is easy and convenient to use, with built-in Chinese navigation and electronic manual
9. Innovative appearance design, electrostatic spraying process is environmentally friendly, easy to clean, and corrosion-resistant
10. Built in thermal high-speed printer and front power switch, making it more convenient for you to use the instrument again
11. RS232 serial port, expandable with optional computer communication, electronic balance communication, and networked management
12. Built in Chinese and English languages, customizable for other languages to facilitate international friends' use
13. Compliant with multiple national standards and applicable to various industries

Compliant with standards

WKT-A9 "Exquisite" Karl Fischer Micro Moisture Analyzer meets the standard:
GB/T 6283-2008 Determination of moisture content in chemical products Karl Fischer method
ASTM E1064-2008 Karl Fischer Coulombic Titration for Determination of Water Content in Organic Liquids
GB/T 7600-1987 Determination of Moisture Content in Operating Transformer Oil (Coulombic Method)
ASTM D4928-00 (2010) Karl Fischer Coulombic Titration for Determination of Water Content in Crude Oil
ASTM D6304-2007 Karl Fischer coulometric titration method for determining water content in petroleum products, lubricants, and additives
ISO 10337-1997 Determination of Moisture in Crude Oil Karl Fischer Coulombic Titration Method
GB/T 11146-2009 Determination of Crude Oil Water Content Karl Fischer Coulombic Titration Method
GB/T 3727-2003 Determination of Trace Water in Ethylene and Propylene for Industrial Use
GB/T 5074-1985 Method for determination of moisture content in coking products by microcoulometry
GB/T 6023-2008 Determination of Trace Water in Butadiene for Industrial Use Karl Fischer Coulombic Method
GB/T 7376-2008 Determination of Trace Moisture in Fluoroalkanes for Industrial Use Karl Fischer Method
GB/T 18619.1-2002 Determination of Water Content in Natural Gas Karl Fischer Coulombic Method
GB/T 18826-2002 Industrial 1,1,1,2-tetrafluoroethane HFC-134a
SH/T 0246-1992 Determination of Water Content in Light Petroleum Products (Electricity Method)
SH/T 0255-1992 Method for determination of moisture content in additives and lubricating oils containing additives (electric method)
ASTM E1064-2008 Karl Fischer Coulombic Titration for Determination of Water Content in Organic Liquids
ASTM D4928-00 (2010) Karl Fischer Coulombic Titration for Determination of Water Content in Crude Oil
ASTM D6304-2007 Karl Fischer coulometric titration method for determining water content in petroleum products, lubricants, and additives;

detailed parameters

PRODUCT MODEL	WKT-A9
Measurement principle	Karl Fischer Coulomb method (electricity method)
measurement speed	40 μ g H₂O/s (automatic control)
measuring range	0.1ug-350mg
Measurement accuracy	When the water content is between 100 μ g of water and 1000 μ g of water, the error is ≤± 2ug. When the water content is above 1000 μ g of water, the error is ≤± 0.2% (excluding injection error), and the standard deviation is ≤ 0.3%
Measurement resolution	0.1 μg H₂O
electrolytic current	0-400mA adjustable
Water content (concentration range)	0%-100%
stirring speed	Stepless touch adjustment
Drift value blank value deduction	Automatic deduction
Special Features	Automatic drift compensation, automatic deduction of environmental and background moisture, optional computer workstation, fault self check prompt
Moisture concentration resolution	0.001
Concentration unit	%The ppm、mg/kg
Display and operation	Color touch screen display operation
sample number	Users can freely set the sample number
Store data	500 items
Printing function	Built in low-energy high-speed thermal printer, 56mm paper width
print contents	Display different types of capacitance based on user measurement formulas and measurement results
Calendar/Time	Display and print out the current time, date, detection time, and date
End point indication	Screen prompt/print output/sound warning/endpoint light indicator
Usage environment	Temperature 2 ℃ -50 ℃, humidity ‹ 90%
Power consumption	≤50W
Host size	350mm300mm170mm
supply voltage	220V 50HZ 150W
weight	8KG

application area

Vicometo brandThe WKT-A9 "Exquisite" Karl Fischer Micro Moisture Analyzer is applied to all industries that require rapid moisture measurement:

liquid	Chemical industry: products suitable for Karl Fischer method determination, such as alcohols, ethers, acids, benzenes, phenols, organic solvents, etc Petroleum and power industry: insulation oil, transformer oil and other oil products Pharmaceutical industry: pharmaceutical raw materials, etc Pesticide industry: emulsifiers, etc Other industries: lithium battery electrolytes, etc
solid	Solid substances with good solubility, such as various inorganic salts and citric acid
gas	Nitrogen SF6、 Natural gas, liquefied gas, fluorocarbons, butadiene and other gases
The following industries require supporting card type heating furnaces for use
insoluble solid	Lithium battery industry, plastic industry, medical industry, ceramic powder, metal powder, etc
Other insoluble solids	Insoluble solids, easily contaminated and cross contaminated samples (lubricating oils, aldehydes and ketones), samples that easily react with Karl Fischer reagent, and samples with slow water release

precautions

1、 Cannot display normally
Please check if the power connection wire, fuse, and power switch of the instrument are functioning properly.
2、 The instrument has been in a stable state all along
1. Evaluate whether the reagent is over iodine (reagent color dark brown opaque or dark). If so, use a 0.5 microliter sampler to extract 0.2-0.4 microliters of water and inject it. Do not use an injector of 50 microliters or larger for injection.
2. Check whether the platinum wire at the bottom of the measuring electrode is connected together, causing a short circuit.
3. Check if the electrode plug is connected incorrectly
3、 The instrument testing is unstable and the shutdown is slow
Please check if the reagent has failed
Please check if there is a lot of moisture adhering to the wall of the electrolytic cell bottle (shake the electrolytic cell bottle)
4、 Open electrolysis without counting
Check if the electrolytic electrode is in good contact, unplug and plug it again, and check if the connecting wire is broken.
5、 Electrolysis does not end
Check if the reagent has expired.
For more common issues, please refer to the manual or call to consult with Vicometo

Complete set of accessories

Can be matched with a card type heating furnace, suitable for rapid determination of trace moisture in insoluble solids such as lithium battery products, plastic particles, etc.

Common accessories and consumables for WKT-A9:


Coulombic method with pyridine containing reagent	Coulombic method without pyridine reagent	One ten thousandth precision balance

solid sampler	deionized water	1000ppm standard sample